Web URL(s): http://www.tandfonline.com/doi/pdf/10.1081/CSS-120000974 Last checked: 10/13/2015 Requires: PDF Reader Access conditions: Item is within a limited-access website
Publication Type:
i
Report
Author(s): Gatson, Lewis A. ;
Locke, Martin A.
Author Affiliation: Gatson: Department of Agronomy, Louisiana State University Agricultural Center, Baton Rouge, LA; Locke: USDA-ARS, Southern Weed Science Unit, Stoneville, MS
Title: Comparison of methodologies for extraction of acifluorfen from soil
Source: Communications in Soil Science and Plant Analysis . Vol. 32, No. 17/18, October 2001, p. 2953-2964.
# of Pages: 12
Publishing Information: New York, NY: Marcel Dekker
Keywords: TIC Keywords: Methodology ; Extraction ; Acifluorfen ; Soils ; Pesticide fate ; EDTA ; Pesticide degradation ; Acids ; Bases
Abstract/Contents: "Efficient methods for extraction of pesticides from soil are necessary for environmental fate studies. This study examined efficiencies of methanol:water solvent systems for recovery of the herbicide acifluorfen [5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoic acid] from soils of different properties. The applicability of supercritical fluid CO2 extraction (SFE) for recovery of acifluorfen was also examined. High recovery (>95%) was obtained over wide range of methanol (40 to 80%) to water compositions. Adding acid, base, EDTA or cation-exchange resin to a 80:20, methanol:water solution offered no improvement. However, EDTA or exchange resin gave slightly higher recoveries of acifluorfen and/or degradation products with incubated soil. Recovery of acifluorfen by SFE required addition of a modifier. Extraction efficiencies equal to the highest obtained with liquid extractions were possible using 40:60, methanol:1 N HCI as a modifier."
Language: English
References: 23
Note: Tables
ASA/CSSA/SSSA Citation (Crop Science -Like - may be incomplete ): Gatson, L. A., and M. A. Locke. 2001. Comparison of methodologies for extraction of acifluorfen from soil. Commun. Soil. Sci. Plant Anal. 32(17/18):p. 2953-2964.
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Web URL(s): http://www.tandfonline.com/doi/pdf/10.1081/CSS-120000974 Last checked: 10/13/2015 Requires: PDF Reader Access conditions: Item is within a limited-access website
MSU catalog number: S 590 .C54
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